{"id":2011,"date":"2020-02-22T15:31:15","date_gmt":"2020-02-22T22:31:15","guid":{"rendered":"https:\/\/www.thinkhighercaregiving.com\/?p=2011"},"modified":"2020-02-22T15:31:15","modified_gmt":"2020-02-22T22:31:15","slug":"think-highers-guide-to-cannabis-distillates","status":"publish","type":"post","link":"https:\/\/thinkhighercaregiving.com\/new-design\/think-highers-guide-to-cannabis-distillates\/","title":{"rendered":"Think Highers Ultimate Guide to Cannabis Distillates"},"content":{"rendered":"
\n
\n
\n
\n
[siteorigin_widget class=”SiteOrigin_Widget_Headline_Widget”][\/siteorigin_widget]<\/div>\n
\n
\n
\n

The extraction and distillation of cannabinoids has come quite a long way since its outbreak just a few years ago.\u00a0\u00a0<\/span><\/p>\n

Simple extraction techniques were well-practiced by many people in the past.The state-of-the-art extraction of today’s world, however, is anything but simple. \"\"<\/span><\/p>\n

Distillation<\/a> is one of the oldest extraction processes. More recently, distillation has begun making waves across cannabis extraction industries. It is speculated that cannabis distillates are the future cannabis extract.<\/span><\/p>\n

What exactly are these cannabis distillates? And more importantly, why is it superior to regular cannabis extract?<\/span><\/p>\n<\/div>\n<\/div>\n<\/div>\n

\n
\n

What Is The Definition Of Distillate?<\/h3>\n
\n

Distillation is scientifically defined as the purification of substances through a collection of heating and then cooling methods. The distillation\u2019s end product is called a <\/span>distillate<\/a>.<\/span><\/p>\n

\"\"Distillation yields a cleaner and purer end concentrate in cannabinoid extracts than most of the other extraction techniques.\u00a0<\/span><\/p>\n

In actual fact, most researchers and enthusiasts seldom refer to the final product of the distillation of cannabinoids process, as the “The Pure.”\u00a0<\/span><\/p>\n

That\u2019s because, even though the cannabinoids have been extracted via a hydrocarbon solvent, the final distillate product is \u201csolvent-free\u201d, meaning it has zero parts-per-million residual solvent.\u00a0<\/span><\/p>\n

\u00a0The distillate products are one of the most effective and diverse types of cannabis and hemp extracts available within the market.<\/span><\/p>\n<\/div>\n<\/div>\n<\/div>\n

\n
\n

What are Cannabinoid Distillates?<\/h3>\n
\n

Top class extraction practitioners use the process of distillation to extract only the specific compounds found in the original material.\u00a0<\/span><\/p>\n

It is possible to majorly distill only CBD or THC from a hemp or cannabis plant, respectively.<\/span><\/p>\n

<\/span><\/p>\n

Cannabis distillates are not as pure as cannabinoid isolates<\/a>, for they are not as refined.<\/span><\/p>\n

Various cannabinoids, valuable molecules and minor contaminants (terpenes and flavonoids) may still be present in cannabis distillates. It can be referred to as a precursor to isolates because it could be further refined even more to isolate a specific cannabinoid.\u00a0<\/span><\/p>\n

Research has found that the cannabinoids profiles found in distillates and remaining beneficial molecules can be highly beneficial for the body.\u00a0<\/span><\/p>\n

For example, CBD Distillates usually contain THC of some amount, which could render it as illegal in some states<\/a>, whereas an isolate-based CBD contains no trace amounts of THC.<\/span><\/p>\n

Moreso, it should be known that most distillates and other extracts, produced for improved THC effectiveness are grown from the raw marijuana plant. <\/span><\/p>\n

In contrast, the CBD distillate is extracted, mostly, from the cultivation of hemp plants.\u00a0<\/span><\/p>\n

Hemp vs. Cannabis<\/h5>\n

\"Hemp<\/p>\n

Cannabidiol(CBD) distillates can be obtained from Marijuana plants from time to time. However, this only increases the possibility that the distillate results in containing high levels of THC. <\/span><\/p>\n

This can have a significant consequences due to how CBD is completely legal for consumption in all 50 states in the US, while THC is not.\u00a0<\/span><\/p>\n

CBD distillate extracted from hemp typically contains about 90 percent or more cannabidiol. The other 10 percent of the distillate is made up of other cannabinoids, and potential unwanted molecules (errors in the distillation process).\u00a0<\/span><\/p>\n

\"CBD

CBD Molecule<\/p><\/div>\n

They are typically the second purest cannabidiol supplements available on the market stock. The enhanced purity offers your end customers the luxury of not consuming much to start enjoying all of its essential benefits.\u00a0<\/span><\/p>\n

Distillates are perfect in the manufacturing of capsules, vape oils, and edibles, tinctures<\/a>, simply because of its purity. Distillates are also often refined even further to make the purest cannabidiol extracts on the market, isolates.<\/span><\/p>\n<\/div>\n<\/div>\n<\/div>\n<\/div>\n<\/div>\n<\/div>\n

\n
\n
[siteorigin_widget class=”SiteOrigin_Widget_Headline_Widget”][\/siteorigin_widget]<\/div>\n
\n
\n

The Process<\/h3>\n
\n

The goal of distillates is to produce a product that has a clean slate<\/a> where we can infuse the desired terpenes for desired effects.<\/span><\/p>\n

The distillation of cannabinoids, as stated above, applies to both CBD derived from hemp, as well as THC derived from Marijuana.<\/span><\/p>\n

There is a reason enthusiasts in the cannabis community sometimes refer to cannabis distillate as “The Pure.”\u00a0 That’s precisely what it is, a product that’s virtually pure cannabinoids.<\/span><\/p>\n<\/div>\n<\/div>\n<\/div>\n

\n
\n

So How Are DISTILLATES Made?<\/h3>\n
\n

Cannabinoids are refined and separated by the process of distillation at the molecular level<\/a>. The goal of making cannabis distillate is to isolate cannabinoids like CBD and THC from unwanted impurities.<\/span><\/p>\n

The whole procedure is made up of several refinement processes. The main steps of the distillation of cannabinoids are explained below;<\/span><\/p>\n

\"\"<\/p>\n

The Initial Crude Extraction of Resin from Hemp plant<\/b><\/h6>\n

The first step of distillation, the same as any cannabinoid extraction, is to extract the cannabinoids from the raw cannabis plant. <\/span><\/p>\n

The extraction and distillation of cannabinoids are incredibly similar, as they both separate compounds.\u00a0<\/span><\/p>\n

In the initial crude oil extraction method, either solvents or physical methods (like rinsing and sifting) are used to separate the compounds.<\/span><\/p>\n

However, there is a large difference between the two.\u00a0<\/span><\/p>\n

Distillation is separating compounds based on boiling points while extraction is separating compounds based on the solubility<\/a> of the extraction solvent.<\/span><\/p>\n

In the cannabis industry, extraction involves the collection of oils from the plant material.<\/span><\/p>\n

\"\"

Oleoresin Credit: Ocpharm.com<\/p><\/div>\n

\u00a0In contrast, distillation describes the process of refining the extracted oil into required constituents, which can be later incorporated into marketable goods.<\/span><\/p>\n

Cannabis crude oil extractions are done by polarity. Remember chemistry class? The saying \u201clike attract likes\u201d? Well that is precisely how solvents work to extract the cannabinoids.<\/span><\/p>\n

Cannabinoids are nonpolar.<\/a> Therefore, nonpolar solvents are used to pull the cannabinoids, leaving behind, unwanted, polar molecules. These polar molecules are things such as chlorophyll and potential water.\u00a0<\/span><\/p>\n

The polar solvents used for extractions ranges from extractor to extractor, like an artist only using a certain type of writing utilize.<\/p>\n

Some of the more polar solvents used are Butane, Propane, & Pentane.<\/p>\n

Alcohols & polar solvents can be used, however more unwanted product results in the final product.<\/p>\n

\"\"<\/p>\n

The first extraction produces a product known as oleoresin<\/a>, which is further refined. <\/span><\/p>\n

The oleoresin, produced in this process, can be summed up as the concentrated cannabinoids, in addition to, all the flavoring ingredients soluble in the particular solvent used, so that it is much closer to the original…odor and flavor.\u00a0<\/span><\/p>\n

Some impurities are still present in the extracted oil – fats, lipids, and several other unwanted compounds. These compounds are removed within the next step, the winterization process.<\/span><\/p>\n

Winterization of Oleoresin to Remove Impurities<\/b><\/h6>\n

Of course, the initial extraction process yields an extract that is full of the desired cannabinoids. But, it also contains many impurities that are unnecessary and could be harmful upon consumption.<\/span><\/p>\n

\u00a0Impurities also prevent the further steps in the distillation processes from making a high quality final product.\u00a0<\/span><\/p>\n

Winterization is conducted to remove unwanted impurities efficiently.\u00a0<\/span><\/p>\n

The winterization process is very similar to baking a chicken:\u00a0 In baking a chicken, the excess grease and juices (aka impurities) drip down into the pan and then thicken when cooled.\u00a0<\/span><\/p>\n

In the winterization process, the crude extract and ethanol solution is passed through a filter. Here, the fats and lipids are removed. The remaining ethanol solution is then typically recovered, done using a rotary evaporation technique.<\/span><\/p>\n

The process starts by mixing the initial crude extract with pure ethanol.\u00a0<\/span><\/p>\n

This solution is placed in a freezing environment for roughly 24 to 48 hours at this point. During the freezing phase, most of the unwanted impurities solidify. <\/span><\/p>\n

\u00a0The extremely cold crude extract and ethanol solution is then passed through a filter.\u00a0 Fats and lipids are caught in the filter, while the cannabnoid rich ethanol passes through. This filtration process is normally performed using a simple buchner funnel.\u00a0<\/span><\/p>\n

Recovery Of Ethanol<\/h6>\n

After the fats, lipids and other minor impurities are filtered out, the ethanol is removed\/recovered. Ethanol removal is typically done using a rotary evaporator.<\/span><\/p>\n

\"\"<\/p>\n

Rotary Evaporation will remove a majority of the ethanol initially added. “One reason that rotary evaporation is favorable for this technique is that the process is efficient with minimal labor. Because the ethanol can be reclaimed once extracted in a rotary evaporator, a manufacturer <\/a><\/span>significantly reduces overhead costs.”\u00a0<\/a>
\n<\/span><\/p>\n

The final product is a resin containing the desired cannabinoids, other minor cannabinoids, terpenes, and antioxidants.<\/p>\n

Decarboxylation of Cannabinoid acids<\/b><\/h6>\n

Cannabinoids found in the cannabis plant are always locked in an acidic form.\u00a0<\/span><\/a><\/p>\n

Cannabinoids generally has more benefits when changed to a more active and stable state. The is accomplished through the decarboxylation process.\u00a0<\/span><\/p>\n

Decarboxylation involves heating the solution to the right temperatures until all of the desired compounds are converted, making them activated.<\/span><\/p>\n

Credit: https:\/\/www.medisenol.com\/science-of-extraction<\/p><\/div>\n

Decarboxylation of the oleoresin is done to minimize the amount of time during the actual distillation step.\u00a0<\/span><\/p>\n

However, decarboxylation can occur during the distillation process.<\/span><\/p>\n

Either done before or after, does not seem to matter, but due to the high temperatures required during distillation, 100% of distillate is decarboxylated. Making them perfect to cook with.<\/span><\/p>\n

Distillation<\/b><\/h6>\n

The distillation process is a separation technique that uses heat, steam, and vacuum pressure to separate compounds in a solution from each other.<\/p>\n

Extractors can collect the compounds individually by influencing the boiling points of each compound.<\/span><\/p>\n

Credit: hightimes.com<\/p><\/div>\n

In a normal cannabinoid distillation, flavonoids, terpenes, and other <\/span>unwanted molecules are removed first, as they contain lower boiling points than cannabinoids.<\/span><\/p>\n

The end product, distillate, is a golden yellow color with a viscosity that is higher than honey.<\/span><\/p>\n

The distillation procedure can be run multiple times to get the distillates further refined.\u00a0<\/span><\/p>\n

It is important to note that there are several different forms of distillations, which are described below.\u00a0<\/span><\/p>\n<\/div>\n<\/div>\n<\/div>\n<\/div>\n<\/div>\n

\n
\n
[siteorigin_widget class=”SiteOrigin_Widget_Headline_Widget”][\/siteorigin_widget]<\/div>\n
\n
\n

Simple Distillation Vs Fractional Distillation. <\/h3>\n
\n
Simple Distillation<\/b><\/h6>\n

Distillations all have similarities in the fact that they both separate mixtures, using similar equipement. However, there are two main types of distillations which distillates are produced by.\u00a0<\/span><\/p>\n

The difference between simple and fractional distillation, at its core, is the number of times that the liquid is vaporized and condensed.\u00a0<\/span><\/p>\n

\"\"<\/p>\n

During simple distillation the liquid condenses once. Therefore a large difference in boiling points of the two liquids must be achieved to make an efficient distillation.\u00a0<\/span><\/p>\n

For example, simple distillation is often used to separate the liquid substance from a solid substance.\u00a0<\/span><\/p>\n

Fractional Distillation<\/b><\/h6>\n

During fractional distillation, two or more cycles of distillation occur.<\/span><\/p>\n

An additional piece of equipment is used during fractional distillation, a fractionating column. This fractionating column acts as an obstruction to the gases.\u00a0<\/span><\/p>\n

\"\"<\/p>\n

As material is heated and boiled, the \u201cnot pure enough\u201d vapors condense on these columns, falling down until it is reheated by other rising gases. This process of heating, condensing, heating, is referred to as rectification. Rectification leads to better separations leading to a purer product.\u00a0<\/span><\/p>\n

The heating and condensing process occurs until the vapor can pass through all the \u201cobstructions\u201d in vapor form where it is eventually collected into a flask.\u00a0<\/span><\/p>\n

Fractional distillation is commonly used when the material being distilled contains molecules with boiling points that are similar to each other.\u00a0<\/a><\/span><\/p>\n

Due to the large number of molecules within the Cannabis plant fractional distillation is the main form used to produce distillate.\u00a0<\/span><\/p>\n

Different Fractional Distillation Setups<\/h5>\n

Credit: Labsociety<\/p><\/div>\n

There are multiple different fractional distillation setups. Again some cater <\/span>to speed while others cater to purity.\u00a0<\/span><\/p>\n

The popular setups for distillate production currently in the industry are:<\/span><\/p>\n